PUBLICATION

Synthesis and biological evaluation of imidazo[1,2-a]pyrimidines and imidazo[1,2-a]pyridines as new inhibitors of the Wnt/β-catenin signaling

Authors
Cosimelli, B., Laneri, S., Ostacolo, C., Sacchi, A., Severi, E., Porcù, E., Rampazzo, E., Moro, E., Basso, G., Viola, G.
ID
ZDB-PUB-140621-1
Date
2014
Source
European Journal of Medicinal Chemistry   83C: 45-56 (Journal)
Registered Authors
Moro, Enrico
Keywords
Colorectal cancer, Imidazo[1,2-a]pyridines, Imidazo[1,2-a]pyrimidines, Signal transduction, Wnt signaling, β-catenin
MeSH Terms
  • Transcription, Genetic/drug effects
  • Cyclin D1/metabolism
  • Animals
  • beta Catenin/genetics
  • beta Catenin/metabolism*
  • Pyrimidines/chemical synthesis*
  • Pyrimidines/chemistry
  • Pyrimidines/pharmacology*
  • Chemistry Techniques, Synthetic
  • Cell Proliferation/drug effects
  • Cyclin B1/metabolism
  • Inhibitory Concentration 50
  • Humans
  • Proto-Oncogene Proteins c-myc/metabolism
  • Pyridines/chemical synthesis*
  • Pyridines/chemistry
  • Pyridines/pharmacology*
  • Wnt Signaling Pathway/drug effects*
  • Zebrafish
  • Glycogen Synthase Kinase 3/metabolism
  • Cell Line, Tumor
PubMed
24950489 Full text @ Eur. J. Med. Chem.
Abstract
Wnt/β-catenin signaling plays an important role in the regulation of embryonic development and tumorigenesis. Since its deregulation results in severe human diseases, especially cancer, the Wnt signaling pathway constitutes a promising platform for pharmacological targeting of cancer. In this study we synthesized a series of imidazo[1,2-a]pyrimidines and imidazo[1,2-a]pyridines and identified some derivatives that were able to inhibit the Wnt/β-catenin signaling pathway in a luciferase reporter assay and cell proliferation in selected cancer cell lines, endowed with APC or β-catenin gene mutations. The most active compounds significantly downregulate the expression of Wnt target genes such as c-myc and cyclin D1. Further studies indicated that these compounds function independently of GSK-3β activity. More importantly, in vivo experiments, carried out on a Wnt-reporter zebrafish model indicate, in particular for compounds 4c and 4i as the most active compounds, an activity comparable to that of the reference compound IWR1, suggesting their potential use not only as small molecule inhibitors of the Wnt/β-catenin signal in Wnt driven cancers, but also in other Wnt-related diseases.
Genes / Markers
Figures
Expression
Phenotype
Mutations / Transgenics
Human Disease / Model
Sequence Targeting Reagents
Fish
Antibodies
Orthology
Engineered Foreign Genes
Mapping